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19. | | GUIOTOKU, M.; HANSEL, F. A.; TAVERNA, L.; WENDLING, I.; MAGALHÃES, W. L. E. Análise sensorial de erva-mate (Ilex paraguariensis St. Hill) utilizando quimiometria e espectroscopia de infravermelho próximo (NIR). In: REUNIÃO ANUAL DA SOCIEDADE BRASILEIRA DE QUÍMICA, 29., 2006, Águas de Lindóia, SP. Anais. Águas de Lindóia: SBQ, 2006. 1 CD-ROM. Biblioteca(s): Embrapa Florestas. |
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20. | | HANSEL, F. A.; RAKOCEVIC, M.; FONTOURA, L.; GUIOTOKU, M.; MAGALHÃES, W. L. E. Perspectiva da espectroscopia de infravermelho próximo (NIR) na análise sensorial de erva-mate chimarrão em pó. In: CONGRESO SUDAMERICANO DE LA YERBA MATE, 4.; REUNIÓN TÉCNICA DE LA YERBA MATE, 4., EXPOSICIÓN DE AGRONEGOCIOS DE LA YERBA MATE, 2., 2006, Posadas. Actas. Posadas: INTA, 2006. p. 78-83. Biblioteca(s): Embrapa Florestas. |
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Registros recuperados : 54 | |
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| Acesso ao texto completo restrito à biblioteca da Embrapa Pantanal. Para informações adicionais entre em contato com cpap.biblioteca@embrapa.br. |
Registro Completo
Biblioteca(s): |
Embrapa Pantanal. |
Data corrente: |
16/04/2013 |
Data da última atualização: |
06/08/2013 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Circulação/Nível: |
A - 1 |
Autoria: |
BERGIER, I.; FREITAS, I. V.; GUIOTOKU, M. |
Afiliação: |
IVAN BERGIER TAVARES DE LIMA, CPAP; ISABEL VINHAL FREITAS, UNIVERSIDADE FEDERAL DE UBERLÂNDIA; MARCELA GUIOTOKU, UNIVERSIDADE FEDERAL DE SANTA CATARINA. |
Título: |
Low vacuum thermochemical conversion of anaerobically digested swine solids. |
Ano de publicação: |
2013 |
Fonte/Imprenta: |
Chemosphere, v. 92, n. 6, p. 714-720, 2013. |
Páginas: |
7 p. |
ISSN: |
0045-6535 |
Idioma: |
Inglês |
Conteúdo: |
This work provides data on the production of biochar from the pyrolysis of the solid phase of swine effluents following anaerobic biodigestion. The study involved the low vacuum thermochemical conversion by environmental scanning electron microscope (ESEM) in a thermoregulated hot-stage tungsten SEM.
The feedstock was characterized by FTIR, ESEM and energy dispersive X-ray analysis (EDS). The charred feedstock at peak temperatures of 300 C, 400 C, 500 C, 600 C, 700 C, and 1000 C were assessed by SEM and EDS. For each pyrolysis experiment, the exhaust gases were monitored by photoacoustic spectroscopy. SEM/EDS indicated that for increasing peak temperature in low vacuum pyrolysis, the mass losses are greater and the proportion of mineral particles such as P, Ca and Mg in the biochar. Photoacoustic spectroscopy showed that low vacuum pyrolysis is responsible for emissions of toxic gases NH3 and SO2 and radiative trace gases, especially N2O above 600 C. |
Palavras-Chave: |
FTIR; Swine manure biochar; X-ray analysis. |
Thesaurus NAL: |
photoacoustic spectroscopy; scanning electron microscopy. |
Categoria do assunto: |
-- |
Marc: |
LEADER 01589naa a2200229 a 4500 001 1955994 005 2013-08-06 008 2013 bl --- 0-- u #d 022 $a0045-6535 100 1 $aBERGIER, I. 245 $aLow vacuum thermochemical conversion of anaerobically digested swine solids. 260 $c2013 300 $a7 p. 520 $aThis work provides data on the production of biochar from the pyrolysis of the solid phase of swine effluents following anaerobic biodigestion. The study involved the low vacuum thermochemical conversion by environmental scanning electron microscope (ESEM) in a thermoregulated hot-stage tungsten SEM. The feedstock was characterized by FTIR, ESEM and energy dispersive X-ray analysis (EDS). The charred feedstock at peak temperatures of 300 C, 400 C, 500 C, 600 C, 700 C, and 1000 C were assessed by SEM and EDS. For each pyrolysis experiment, the exhaust gases were monitored by photoacoustic spectroscopy. SEM/EDS indicated that for increasing peak temperature in low vacuum pyrolysis, the mass losses are greater and the proportion of mineral particles such as P, Ca and Mg in the biochar. Photoacoustic spectroscopy showed that low vacuum pyrolysis is responsible for emissions of toxic gases NH3 and SO2 and radiative trace gases, especially N2O above 600 C. 650 $aphotoacoustic spectroscopy 650 $ascanning electron microscopy 653 $aFTIR 653 $aSwine manure biochar 653 $aX-ray analysis 700 1 $aFREITAS, I. V. 700 1 $aGUIOTOKU, M. 773 $tChemosphere$gv. 92, n. 6, p. 714-720, 2013.
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